23.
Pick out the wrong statement.

24.
A sampling tube known as a thief, which has two concentric and close fitting tubes with matching holes or opening, is used for the sampling of

25.
Loss on ignition (LOI) of iron ore is determined by finiding the loss in weight of the sample by heating it first to 500°C for 5 minutes followed by its heating at . . . . . . . . °C, for 30 minutes.

26.
Determination of methane present in coke oven gas by orsat apparatus, it is completely oxidised in contact with CuO to CO2 and H2O at a temperature of, . . . . . . . . . °C.

27.
Determination of alumina (AI2O3) in iron ore is based on the selective formation of AIPO4 from its acidic solution (with cone, HCl) by the addition of

28.
Determination of ash content of coal during its proximate analysis, the temperature of weighed coal sample is raised to 400 - 500°C in half an hour and maintained at the same level for further half an hour. The temperature is then raised to . . . . . . . . °C at which the sample is heated for one more hour before weighing it.

29.
Eschka mixture used in total sulphur determination in coal comprises of a mixture of . . . . . . . . in 2 : 1 ratio by weight.