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1
Determination of phosphorous content of iron & steel is done by bringing phosphorous into solution and then finding it by the . . . . . . . . method.
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Answer & Solution
Answer: Option D
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2
Temperature used in the determination of volatile matter of coal is . . . . . . . . °C.
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Answer: Option C
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3
During volatile matter content determination, air dried coal sample is heated for 7 minutes at a constant temperature of . . . . . . . . °C.
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Answer & Solution
Answer: Option B
Solution:
The correct answer is Option B: 925 °C.

Let's understand why we do this test and what it means for coal.

Imagine coal as a kind of rock that can burn. When we talk about volatile matter in coal, we are referring to the parts of the coal that turn into gases or vapors when heated strongly, but without any air (oxygen) present. It's like heating wood in an enclosed space; some gases come out before the wood itself starts to burn.

Why is this important?
Knowing the volatile matter content helps us understand many things about coal:
1. Ignition and Burning: Coal with high volatile matter usually ignites more easily and burns with a longer, more luminous flame. Coal with low volatile matter is harder to ignite.
2. Smoke Production: Higher volatile matter can lead to more smoke during combustion.
3. Industrial Use: Different industries need different types of coal. For example, in coke making (for steel production), the volatile matter content is very critical.
4. Coal Classification: It's one of the key factors used to classify different ranks of coal (like lignite, bituminous, anthracite).

How do we determine it?
To find the volatile matter content, we follow a standard procedure:
1. A small, carefully air-dried coal sample is weighed.
2. This sample is then placed in a special crucible with a lid (to keep air out).
3. The crucible is then heated in a furnace for a specific time and at a specific temperature.
4. The standard method requires heating the sample for exactly 7 minutes at a constant temperature of 925 °C (plus or minus a small allowance).
5. After heating, the sample is cooled and weighed again. The weight loss (after accounting for moisture) represents the volatile matter that escaped as gas.

The temperature of 925 °C is chosen because it ensures that most of the volatile components are driven off, but the coal itself doesn't undergo significant decomposition beyond that point in the given time. This specific temperature and time are part of the standard test method to ensure consistent and comparable results worldwide.
4
For hydrogen analysis in blast furnace, gas by Orsat apparatus, it is completely oxidised in contact with CuO to H2O at a-temperature of about . . . . . . . . °C.
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Answer & Solution
Answer: Option B
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5
Cuprous chloride solution is used in orsat apparatus for selectively absorbing carbon monoxide. However, it is capable of absorbing . . . . . . . . also.
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Answer & Solution
Answer: Option D
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6
Ammonia present in coke oven gas is determined by passing its measured volume through the standard solution of
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Answer & Solution
Answer: Option A
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7
During dissolution of iron from iron ore in acid solution, the rate of dissolution is accelerated by the addition of little amount of . . . . . . . . which reduces ferric iron to ferrous state.
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Answer & Solution
Answer: Option C
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8
For moisture determination during proximate analysis of coal, -72 mesh coal (2 - 10 gms) is heated between 105 to 110°C
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Answer: Option D
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9
Determination of volatile matter in coal, during its proxiinate analysis requires heating of coal sample.
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Answer: Option C
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10
Calorific value of fuel gases is not determined by the . . . . . . . . calorimeter,
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Answer & Solution
Answer: Option A
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